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8
Chromatogram

2-Methyl-3-(3,4-dihydroxy-phenyl)-DL-alanine

CHIRALPAK® ZWIX(+) (150 x 3mm 3µm)

50mM formic acid + 25mM diethylamine in methanol / acetonitrile / water = 49 / 49 / 2
161
Chromatogram

2-Phenoxypropionic acid

CHIRALPAK® IB-3 (50 x 4.6mm 3µm)

n-hexane / chloroform / ethanol / trifluoroacetic acid = 68 / 30 / 2 / 0.1
275
Chromatogram

2-Phenoxypropionic acid

CHIRALPAK® IB (250 x 4.6mm 5µm)

n-hexane / dimethoxymethane / trifluoroacetic acid = 75 / 25 / 0.1
553
Chromatogram

2-Phenoxypropionic acid

CHIRALCEL® OD-3 (50 x 4.6mm 3µm)

n-hexane / 2-propanol / trifluoroacetic acid = 90 / 10 / 0.1
615
Chromatogram

2-Phenoxypropionic acid

CHIRALPAK® AD-H (250 x 4.6mm 5µm)

n-hexane / 2-propanol / trifluoroacetic acid = 80 / 20 / 0.1
616
Chromatogram

2-Phenoxypropionic acid

CHIRALCEL® OJ-H (250 x 4.6mm 5µm)

n-hexane / 2-propanol / trifluoroacetic acid = 98 / 2 / 0.1
859
Chromatogram

2-Phenoxypropionic acid

CHIRALPAK® AGP (100 x 4mm 5µm)

10mM NH4OAc aq. pH4.5 / methanol = 95 / 5
955
Chromatogram

2-Phenoxypropionic acid

CHIRALPAK® QN-AX (150 x 4.6mm 5µm)

methanol / 0.2mM acetic acid aq. pHa6.0 = 80 / 20
1174
Chromatogram

2-Phenoxypropionic acid

CHIRALPAK® QN-AX (150 x 4.6mm 5µm)

methanol / acetic acid / NH4OAc = 98 / 2 / 0.5
1175
Chromatogram

2-Phenoxypropionic acid

CHIRALPAK® QD-AX (150 x 4.6mm 5µm)

acetonitrile / acetic acid = 97 / 3
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