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1028
Chromatogram

7,8,9,10-Tetrahydrobenzo[a]pyren-7-ol

CHIRALPAK® AY-H (150 x 4.6mm 5µm)

acetonitrile / 2-propanol = 95 / 5
1050
Chromatogram

7,8,9,10-Tetrahydrobenzo[a]pyren-7-ol

CHIRALCEL® OJ-3 (150 x 4.6mm 3µm)

acetonitrile = 100
1051
Chromatogram

7,8,9,10-Tetrahydrobenzo[a]pyren-7-ol

CHIRALCEL® OJ-3 (150 x 4.6mm 3µm)

methanol = 100
1106
Chromatogram

7,8,9,10-Tetrahydrobenzo[a]pyren-7-ol

CHIRALCEL® OJ-H (150 x 4.6mm 5µm)

methanol = 100
179
Chromatogram

9,10-Dihydro-2-methyl-4H-benzo-[5,6] cyclohept[1,2-d]oxazol-4-ol

CHIRALPAK® IA-3 (150 x 4.6mm 3µm)

n-hexane / 2-propanol / ethanolamine = 85 / 15 / 0.1
180
Chromatogram

9,10-Dihydro-2-methyl-4H-benzo-[5,6] cyclohept[1,2-d]oxazol-4-ol

CHIRALPAK® IA-3 (150 x 4.6mm 3µm)

n-hexane / dichloromethane / ethanol / ethanolamine = 50 / 50 / 2 / 0.1
285
Chromatogram

9,10-Dihydro-2-methyl-4H-benzo-[5,6] cyclohept[1,2-d]oxazol-4-ol

CHIRALPAK® IC (250 x 4.6mm 5µm)

n-heptane / ethanol / diethylamine = 85 / 15 / 0.1
286
Chromatogram

9,10-Dihydro-2-methyl-4H-benzo-[5,6] cyclohept[1,2-d]oxazol-4-ol

CHIRALPAK® IC (250 x 4.6mm 5µm)

n-hexane / ethyl acetate / ethanolamine = 60 / 40 / 0.1
287
Chromatogram

9,10-Dihydro-2-methyl-4H-benzo-[5,6] cyclohept[1,2-d]oxazol-4-ol

CHIRALPAK® IC (250 x 4.6mm 5µm)

n-hexane / tetrahydrofuran / diethylamine = 85 / 15 / 0.1
624
Chromatogram

9,10-Dihydro-2-methyl-4H-benzo-[5,6] cyclohept[1,2-d]oxazol-4-ol

CHIRALCEL® OD-H (250 x 4.6mm 5µm)

n-heptane / ethanol / diethylamine = 70 / 30 / 0.1
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