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1491
Chromatogram

Alogliptin

CHIRALPAK® IF-3 (250 x 4.6mm 3µm)

ethanol / methanol / diethylamine = 70 / 30 / 0.1
1549
Chromatogram

Alogliptin

CROWNPAK® CR-I(+) (150 x 3mm 5µm)

perchloric acid aq. pH1.0 / acetonitrile = 80 / 20
181
Chromatogram

alpha-(2,4-Dichlorophenyl)-1H-imidazole-1-ethanol

CHIRALPAK® IA-3 (50 x 4.6mm 3µm)

n-hexane / ethanol / ethanolamine = 80 / 20 / 0.1
290
Chromatogram

alpha-(2,4-Dichlorophenyl)-1H-imidazole-1-ethanol

CHIRALPAK® IA (250 x 4.6mm 5µm)

n-heptane / 2-propanol / diethylamine = 85 / 15 / 0.1
291
Chromatogram

alpha-(2,4-Dichlorophenyl)-1H-imidazole-1-ethanol

CHIRALPAK® IA (250 x 4.6mm 5µm)

toluene / n-hexane / ethanol / diethylamine = 70 / 25 / 5 / 0.1
292
Chromatogram

alpha-(2,4-Dichlorophenyl)-1H-imidazole-1-ethanol

CHIRALPAK® IC (250 x 4.6mm 5µm)

n-heptane / 2-propanol / diethylamine = 85 / 15 / 0.1
718
Chromatogram

alpha-(2,4-Dichlorophenyl)-1H-imidazole-1-ethanol

CHIRALPAK® IA-3 (50 x 4.6mm 3µm)

20mM NH4CO3 aq. pH9.0 / acetonitrile = 30 / 70
770
Chromatogram

alpha-(2,4-Dichlorophenyl)-1H-imidazole-1-ethanol

CHIRALPAK® AS-3R (150 x 4.6mm 3µm)

20mM NH4CO3 aq. pH9.0 / acetonitrile = 60 / 40
975
Chromatogram

alpha-(2,4-Dichlorophenyl)-1H-imidazole-1-ethanol

CHIRALPAK® IA (250 x 4.6mm 5µm)

methanol / diethylamine = 100 / 0.1
1054
Chromatogram

alpha-(2,4-Dichlorophenyl)-1H-imidazole-1-ethanol

CHIRALPAK® AD-3 (50 x 4.6mm 3µm)

methanol / diethylamine = 100 / 0.1
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