APPLICATION ID 1556

Metaraminol

COMPOUND IDENTIFICATION

Compound Name Metaraminol
Metaraminol

CHROMATOGRAM

Chromatogram

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CROWNPAK® CR-I(+)

150 x 3mm / 5µm

Mobile Phase Composition

perchloric acid aq. pH1.0 / acetonitrile = 80 / 20

Chromatographic Mode

Reverse Phase

Flow rate (ml/min)

0.4

Injection amount (mg)

0.02

Temperature (°C)

10

Pressure (MPa)

Detection

UV 275 nm

Elution order

Diastereomer, Diastereomer, API, Enantiomer

No.

Rt

K’

1

3.86

0.8

2

4.37

1.03

3

4.84

1.25

4

7.33

2.41

Alpha Value

Resolution

1 - 2

1.3

1.57

2 - 3

1.21

2.25

3 - 4

1.93

5.63

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