APPLICATION ID 1697

Darunavir

COMPOUND IDENTIFICATION

Compound Name Darunavir
Darunavir

CHROMATOGRAM

Chromatogram

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® IE-3

250 x 4.6mm / 3µm

Mobile Phase Composition

n-hexane / ethanol / diethylamine = 70 / 30 / 0.1

Chromatographic Mode

Normal Phase

Flow rate (ml/min)

1.0

Injection amount (mg)

Temperature (°C)

25

Pressure (MPa)

Detection

UV 265 nm

Elution order

No.

Rt

K’

1

14.9

2

16.4

3

17.8

4

22.4

Alpha Value

Resolution

1 - 2

1.7

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