APPLICATION ID 1746

Saxagliptin

COMPOUND IDENTIFICATION

Compound Name Saxagliptin
Saxagliptin

CHROMATOGRAM

Chromatogram

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® ID

250 x 4.6mm / 5µm

Mobile Phase Composition

n-hexane / ethanol / 1,4-dioxane / isopropylamine = 60 / 20 / 20 / 0.1

Chromatographic Mode

Normal Phase

Flow rate (ml/min)

1.0

Injection amount (mg)

Temperature (°C)

25

Pressure (MPa)

Detection

UV 225 nm

Elution order

No.

Rt

K’

1

7.5

2

8.8

3

10.4

4

11.1

Alpha Value

Resolution

1 - 2

3.3

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