APPLICATION ID 381

Mitiglinide (racemic)

COMPOUND IDENTIFICATION

Compound Name Mitiglinide (racemic)
Mitiglinide (racemic)

CHROMATOGRAM

Chromatogram

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® IA

250 x 4.6mm / 5µm

Mobile Phase Composition

methyl tert-butyl ether / methanol / trifluoroacetic acid = 60 / 40 / 0.3

Chromatographic Mode

Normal Phase
Primary screening solvent (Immobilised CSP)

Flow rate (ml/min)

0.5

Injection amount (mg)

Temperature (°C)

25

Pressure (MPa)

Detection

UV 215 nm

Elution order

No.

Rt

K’

1

7.83

0.31

2

9.02

0.5

Alpha Value

Resolution

1 - 2

1.65

2.73

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