APPLICATION ID 398

N-FMOC-DL-Leucine

COMPOUND IDENTIFICATION

Compound Name N-FMOC-DL-Leucine
N-FMOC-DL-Leucine

CHROMATOGRAM

Chromatogram

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® IB

250 x 4.6mm / 5µm

Mobile Phase Composition

n-hexane / 2-propanol / trifluoroacetic acid = 90 / 10 / 0.1

Chromatographic Mode

Normal Phase
Primary screening solvent (Immobilised CSP)

Flow rate (ml/min)

1

Injection amount (mg)

0.005

Temperature (°C)

25

Pressure (MPa)

Detection

UV 254 nm

Elution order

No.

Rt

K’

1

9.8

2.33

2

11.57

2.94

Alpha Value

Resolution

1 - 2

1.26

3.03

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