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1542
Chromatogram

Tramadol

CHIRALPAK® ID (250 x 4.6mm 5µm)

n-hexane / dichloromethane / 2-propanol / diethylamine = 80 / 10 / 10 / 0.1
1543
Chromatogram

Tramadol

CHIRALPAK® AD-RH (150 x 4.6mm 5µm)

10mM ammonium bicarbonate aq. pH8.5 / acetonitrile = 65 / 35
251
Chromatogram

trans-2-Phenylcyclopropane-1-carboxylic acid

CHIRALPAK® IB-3 (50 x 4.6mm 3µm)

n-hexane / ethyl acetate / trifluoroacetic acid = 80 / 20 / 0.1
453
Chromatogram

trans-2-Phenylcyclopropane-1-carboxylic acid

CHIRALPAK® IA (250 x 4.6mm 5µm)

hexane / ethanol / trifluoroacetic acid = 85 / 15 / 0.1
454
Chromatogram

trans-2-Phenylcyclopropane-1-carboxylic acid

CHIRALPAK® IB (250 x 4.6mm 5µm)

n-hexane / chloroform / trifluoroacetic acid = 50 / 50 / 0.1
593
Chromatogram

trans-2-Phenylcyclopropane-1-carboxylic acid

CHIRALCEL® OD-3 (50 x 4.6mm 3µm)

n-hexane / 2-propanol / trifluoroacetic acid = 90 / 10 / 0.1
799
Chromatogram

trans-2-Phenylcyclopropane-1-carboxylic acid

CHIRALCEL® OD-3R (150 x 4.6mm 3µm)

formic acid aq. pH2.0 / acetonitrile = 60 / 40
961
Chromatogram

trans-2-Phenylcyclopropane-1-carboxylic acid

CHIRALPAK® QN-AX (150 x 4.6mm 5µm)

methanol / 0.2mM acetic acid aq. pHa6.0 = 80 / 20
138
Chromatogram

trans-4-Hydroxy-DL-proline

CHIRALPAK® ZWIX(+) (150 x 3mm 3µm)

50mM formic acid + 25mM diethylamine in methanol / water = 98 / 2
139
Chromatogram

trans-4-Hydroxy-DL-proline

CHIRALPAK® ZWIX(-) (150 x 3mm 3µm)

50mM formic acid + 25mM diethylamine in methanol / acetonitrile / water = 49 / 49 / 2
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