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180
Chromatogram

9,10-Dihydro-2-methyl-4H-benzo-[5,6] cyclohept[1,2-d]oxazol-4-ol

CHIRALPAK® IA-3 (150 x 4.6mm 3µm)

n-hexane / dichloromethane / ethanol / ethanolamine = 50 / 50 / 2 / 0.1
285
Chromatogram

9,10-Dihydro-2-methyl-4H-benzo-[5,6] cyclohept[1,2-d]oxazol-4-ol

CHIRALPAK® IC (250 x 4.6mm 5µm)

n-heptane / ethanol / diethylamine = 85 / 15 / 0.1
286
Chromatogram

9,10-Dihydro-2-methyl-4H-benzo-[5,6] cyclohept[1,2-d]oxazol-4-ol

CHIRALPAK® IC (250 x 4.6mm 5µm)

n-hexane / ethyl acetate / ethanolamine = 60 / 40 / 0.1
287
Chromatogram

9,10-Dihydro-2-methyl-4H-benzo-[5,6] cyclohept[1,2-d]oxazol-4-ol

CHIRALPAK® IC (250 x 4.6mm 5µm)

n-hexane / tetrahydrofuran / diethylamine = 85 / 15 / 0.1
624
Chromatogram

9,10-Dihydro-2-methyl-4H-benzo-[5,6] cyclohept[1,2-d]oxazol-4-ol

CHIRALCEL® OD-H (250 x 4.6mm 5µm)

n-heptane / ethanol / diethylamine = 70 / 30 / 0.1
717
Chromatogram

9,10-Dihydro-2-methyl-4H-benzo-[5,6] cyclohept[1,2-d]oxazol-4-ol

CHIRALPAK® IA-3 (50 x 4.6mm 3µm)

20mM NH4CO3 aq. pH9.0 / acetonitrile = 70 / 30
769
Chromatogram

9,10-Dihydro-2-methyl-4H-benzo-[5,6] cyclohept[1,2-d]oxazol-4-ol

CHIRALPAK® AD-3R (50 x 4.6mm 3µm)

20mM NH4CO3 aq. pH9.0 / acetonitrile = 60 / 40
814
Chromatogram

9,10-Dihydro-2-methyl-4H-benzo-[5,6] cyclohept[1,2-d]oxazol-4-ol

CHIRALCEL® OJ-RH (150 x 4.6mm 5µm)

20mM borate buffer pH9.0 / acetonitrile = 60 / 40
964
Chromatogram

9,10-Dihydro-2-methyl-4H-benzo-[5,6] cyclohept[1,2-d]oxazol-4-ol

CHIRALPAK® IA-3 (150 x 4.6mm 3µm)

acetonitrile / ethanolamine = 100 / 0.1
989
Chromatogram

9,10-Dihydro-2-methyl-4H-benzo-[5,6] cyclohept[1,2-d]oxazol-4-ol

CHIRALPAK® AY-3 (150 x 4.6mm 3µm)

ethanol / diethylamine = 100 / 0.1
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