COMPOUND IDENTIFICATION
Compound name
- Aprepitant
CHROMATOGRAM
ANALYTICAL REPORT
|
Column Trade Name (Column size / Particle size) |
CHIRALPAK® AD-3 (4.6 x 250 mm 3 µm) |
|---|---|
| Chromatographic Mode | Normal Phase |
| Mobile Phase Composition | n-hexane / 2-propanol = 92 / 8 |
| Flow rate (mL/min) | 0.7 | Temperature (℃) | 30 |
|---|---|---|---|
| Injection Volume (µL) | 0.01 (mg) | Sample Concentration | |
| Detection | UV-VIS 210 nm | ||
| Elution Order | |||
| No. | Rt | K' |
|---|---|---|
| 1 | 8.1 | 0.90 |
| 2 | 9.2 | 1.14 |
| 3 | 10.2 | 1.37 |
| 4 | 12.4 | 1.88 |
| 5 | 15.6 | 2.65 |
| Alpha Value | Resolution | |
|---|---|---|
| 1 - 2 | 1.27 | 3.15 |
| 2 - 3 | 1.21 | 2.64 |
| 3 - 4 | 1.37 | 4.98 |
| 4 - 5 | 1.40 | 5.95 |