COMPOUND IDENTIFICATION
Compound name
- Saxagliptin
CHROMATOGRAM
ANALYTICAL REPORT
|
Column Trade Name (Column size / Particle size) |
CROWNPAK® CR-I(+) (3 x 150 mm 5 µm) |
|---|---|
| Chromatographic Mode | Reverse Phase |
| Mobile Phase Composition | perchloric acid aq. pH1.0 / acetonitrile = 90 / 10 |
| Flow rate (mL/min) | 0.4 | Temperature (℃) | 40 |
|---|---|---|---|
| Injection Volume (µL) | 0.005 (mg) | Sample Concentration | |
| Detection | UV-VIS 220 nm | ||
| Elution Order | Enantiomer, API | ||
| No. | Rt | K' |
|---|---|---|
| 1 | 4.4 | 1.06 |
| 2 | 5.2 | 1.42 |
| Alpha Value | Resolution | |
|---|---|---|
| 1 - 2 | 1.34 | 2.94 |