COMPOUND IDENTIFICATION
Compound name
- Carfilzomib
CHROMATOGRAM
ANALYTICAL REPORT
|
Column Trade Name (Column size / Particle size) |
CHIRALPAK® IA-3 (4.6 x 250 mm 3 µm) |
|---|---|
| Chromatographic Mode | Normal Phase |
| Mobile Phase Composition | n-hexane / methyl tert-butyl ether / methanol = 50 / 40 / 10 |
| Flow rate (mL/min) | 1.0 | Temperature (℃) | 30 |
|---|---|---|---|
| Injection Volume (µL) | Sample Concentration | ||
| Detection | UV-VIS 210 nm | ||
| Elution Order | |||
| No. | Rt | K' |
|---|---|---|
| 1 | 4.6 | - |
| 2 | 6.2 | |
| 3 | 7.0 | |
| 4 | 8.5 |
| Alpha Value | Resolution | |
|---|---|---|
| 1 - 2 | - | 5.30 |
| 2 - 3 | 2.80 | |
| 3 - 4 | 3.90 |