COMPOUND IDENTIFICATION
Compound name
- Saxagliptin
CHROMATOGRAM
ANALYTICAL REPORT
|
Column Trade Name (Column size / Particle size) |
CHIRALPAK® IG-3 (4.6 x 250 mm 3 µm) |
|---|---|
| Chromatographic Mode | Polar Phase |
| Mobile Phase Composition | ethanol / acetonitrile / isopropylamine = 20 / 80 / 0.1 |
| Flow rate (mL/min) | 1.0 | Temperature (℃) | 25 |
|---|---|---|---|
| Injection Volume (µL) | Sample Concentration | ||
| Detection | UV-VIS 220 nm | ||
| Elution Order | |||
| No. | Rt | K' |
|---|---|---|
| 1 | 6.2 | - |
| 2 | 11.8 | |
| 3 | 13.1 | |
| 4 | 15.1 |
| Alpha Value | Resolution | |
|---|---|---|
| 1 - 2 | - | 14.10 |
| 2 - 3 | 2.30 | |
| 3 - 4 | 2.50 |