COMPOUND IDENTIFICATION
Compound name
- DL-Leucine
CHROMATOGRAM
ANALYTICAL REPORT
|
Column Trade Name (Column size / Particle size) |
CROWNPAK® CR-I(+) (3 x 150 mm 5 µm) |
|---|---|
| Chromatographic Mode | HILIC |
| Mobile Phase Composition | acetonitrile / water / trifluoroacetic acid = 96 / 4 / 0.5 |
| Flow rate (mL/min) | 0.4 | Temperature (℃) | 30 |
|---|---|---|---|
| Injection Volume (µL) | Sample Concentration | ||
| Detection | LC-MS | ||
| Elution Order | |||
| No. | Rt | K' |
|---|---|---|
| 1 | 1.9 | - |
| 2 | 7.5 |
| Alpha Value | Resolution | |
|---|---|---|
| 1 - 2 | - | 15.82 |
References；
Extra-facile chiral separation of amino acid enantiomers by LC-TOFMS analysis
Yutaka Konya, Takeshi Bamba, Eiichiro Fukusaki
Volume 121, Issue 3, March 2016, Pages 349-353