COMPOUND IDENTIFICATION
Compound name
- Sitagliptin (racemic)
CHROMATOGRAM
ANALYTICAL REPORT
|
Column Trade Name (Column size / Particle size) |
CHIRALPAK® IC-3 (4.6 x 150 mm 3 µm) |
|---|---|
| Chromatographic Mode | Normal Phase |
| Mobile Phase Composition | n-hexane / 2-propanol / ethylenediamine = 50 / 50 / 0.1 |
| Flow rate (mL/min) | 1 | Temperature (℃) | 40 |
|---|---|---|---|
| Injection Volume (µL) | Sample Concentration | ||
| Detection | UV-VIS 265 nm | ||
| Elution Order | |||
| No. | Rt | K' |
|---|---|---|
| 1 | 6.9 | 2.84 |
| 2 | 8.4 | 3.67 |
| Alpha Value | Resolution | |
|---|---|---|
| 1 - 2 | 1.29 | 2.62 |