COMPOUND IDENTIFICATION
Compound name
- Vildagliptin (racemic)
CHROMATOGRAM
ANALYTICAL REPORT
|
Column Trade Name (Column size / Particle size) |
CHIRALPAK® IC (4.6 x 250 mm 5 µm) |
|---|---|
| Chromatographic Mode | Polar Phase |
| Mobile Phase Composition | ethanol / diethylamine = 100 / 0.1 |
| Flow rate (mL/min) | 0.5 | Temperature (℃) | 25 |
|---|---|---|---|
| Injection Volume (µL) | Sample Concentration | ||
| Detection | UV-VIS 210 nm | ||
| Elution Order | |||
| No. | Rt | K' |
|---|---|---|
| 1 | 11.3 | 0.89 |
| 2 | 14.3 | 1.39 |
| Alpha Value | Resolution | |
|---|---|---|
| 1 - 2 | 1.57 | 4.02 |