COMPOUND IDENTIFICATION
Compound name
- Metaraminol
CHROMATOGRAM
ANALYTICAL REPORT
|
Column Trade Name (Column size / Particle size) |
CROWNPAK® CR-I(+) (3 x 150 mm 5 µm) |
|---|---|
| Chromatographic Mode | Reverse Phase |
| Mobile Phase Composition | perchloric acid aq. pH1.0 / acetonitrile = 80 / 20 |
| Flow rate (mL/min) | 0.4 | Temperature (℃) | 10 |
|---|---|---|---|
| Injection Volume (µL) | 0.02 (mg) | Sample Concentration | |
| Detection | UV-VIS 275 nm | ||
| Elution Order | Diastereomer, Diastereomer, API, Enantiomer | ||
| No. | Rt | K' |
|---|---|---|
| 1 | 3.9 | 0.80 |
| 2 | 4.4 | 1.03 |
| 3 | 4.8 | 1.25 |
| 4 | 7.3 | 2.41 |
| Alpha Value | Resolution | |
|---|---|---|
| 1 - 2 | 1.30 | 1.57 |
| 2 - 3 | 1.21 | 2.25 |
| 3 - 4 | 1.93 | 5.63 |