COMPOUND IDENTIFICATION
Compound name
- DL-Citrulline
CHROMATOGRAM
ANALYTICAL REPORT
|
Column Trade Name (Column size / Particle size) |
CROWNPAK® CR-I(+) (3 x 150 mm 5 µm) |
|---|---|
| Chromatographic Mode | HILIC |
| Mobile Phase Composition | acetonitrile / ethanol / water / trifluoroacetic acid = 80 / 15 / 5 / 0.5 |
| Flow rate (mL/min) | 0.4 | Temperature (℃) | 30 |
|---|---|---|---|
| Injection Volume (µL) | Sample Concentration | ||
| Detection | LC-MS | ||
| Elution Order | |||
| No. | Rt | K' |
|---|---|---|
| 1 | 1.6 | - |
| 2 | 3.4 |
| Alpha Value | Resolution | |
|---|---|---|
| 1 - 2 | - | 10.82 |
References；
Novel high-throughput and widely-targeted liquid chromatography–time of flight mass spectrometry method for d-amino acids in foods
Yutaka Konya, Moyu Taniguchi, Eiichiro Fukusaki
Volume 123, Issue 1, January 2017, Pages 126-133