COMPOUND IDENTIFICATION
Compound name
- Linagliptin
CHROMATOGRAM
ANALYTICAL REPORT
|
Column Trade Name (Column size / Particle size) |
CHIRALPAK® IG-3 (4.6 x 250 mm 3 µm) |
|---|---|
| Chromatographic Mode | Polar Phase |
| Mobile Phase Composition | methanol / acetonitrile / ethylenediamine = 80 / 20 / 0.1 |
| Flow rate (mL/min) | 1.0 | Temperature (℃) | 40 |
|---|---|---|---|
| Injection Volume (µL) | 10 | Sample Concentration |
1.0 mg/mL in MeOH |
| Detection | UV-VIS 295 nm | ||
| Elution Order | |||
| No. | Rt | K' |
|---|---|---|
| 1 | 7.2 | - |
| 2 | 8.6 |
| Alpha Value | Resolution | |
|---|---|---|
| 1 - 2 | - | 2.50 |
- Comment
- Analyte was disolvoed Metformin 340 mg and Linaglipin 1.0 mg/mL in MeOH 1mL.