APPLICATION ID 1494

Aprepitant

COMPOUND IDENTIFICATION

Compound Name Aprepitant
Aprepitant

CHROMATOGRAM

Chromatogram

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® AD-3

250 x 4.6mm / 3µm

Mobile Phase Composition

n-hexane / 2-propanol = 92 / 8

Chromatographic Mode

Normal Phase
Coated CSP

Flow rate (ml/min)

0.7

Injection amount (mg)

0.01

Temperature (°C)

30

Pressure (MPa)

Detection

UV 210 nm

Elution order

No.

Rt

K’

1

8.13

0.9

2

9.15

1.14

3

10.16

1.37

4

12.36

1.88

5

15.63

2.65

Alpha Value

Resolution

1 - 2

1.27

3.15

2 - 3

1.21

2.64

3 - 4

1.37

4.98

4 - 5

1.4

5.95

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