APPLICATION ID 1499

Celecoxib

COMPOUND IDENTIFICATION

Compound Name Celecoxib
Celecoxib

CHROMATOGRAM

Chromatogram

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® IA-3

150 x 4.6mm / 3µm

Mobile Phase Composition

n-hexane / 2-propanol / diethylamine = 92 / 8 / 0.1

Chromatographic Mode

Normal Phase
Primary screening solvent (Immobilised CSP)

Flow rate (ml/min)

1

Injection amount (mg)

0.01

Temperature (°C)

25

Pressure (MPa)

Detection

UV 255 nm

Elution order

No.

Rt

K’

1

10.76

4.98

2

11.65

5.47

3

14.49

7.05

Alpha Value

Resolution

1 - 2

1.1

1.78

2 - 3

1.29

4.88

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