APPLICATION ID 1501

Cinacalcet

COMPOUND IDENTIFICATION

Compound Name Cinacalcet
Cinacalcet

CHROMATOGRAM

Chromatogram

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® IA-3

250 x 4.6mm / 3µm

Mobile Phase Composition

n-hexane / ethanol / trifluoroacetic acid = 96 / 4 / 0.1

Chromatographic Mode

Normal Phase
Primary screening solvent (Immobilised CSP)

Flow rate (ml/min)

1

Injection amount (mg)

0.0025

Temperature (°C)

40

Pressure (MPa)

Detection

UV 225 nm

Elution order

Enantiomer, API

No.

Rt

K’

1

10.78

2.59

2

12.17

3.06

Alpha Value

Resolution

1 - 2

1.18

2.7

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