APPLICATION ID 1549

Alogliptin

COMPOUND IDENTIFICATION

Compound Name Alogliptin
Alogliptin

CHROMATOGRAM

Chromatogram

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CROWNPAK® CR-I(+)

150 x 3mm / 5µm

Mobile Phase Composition

perchloric acid aq. pH1.0 / acetonitrile = 80 / 20

Chromatographic Mode

Reverse Phase

Flow rate (ml/min)

0.5

Injection amount (mg)

0.01

Temperature (°C)

25

Pressure (MPa)

Detection

UV 275 nm

Elution order

No.

Rt

K’

1

9.75

4.67

2

13.85

7.05

Alpha Value

Resolution

1 - 2

1.51

5.74

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