APPLICATION ID 1658

Alogliptin

COMPOUND IDENTIFICATION

Compound Name Alogliptin
Alogliptin

CHROMATOGRAM

Chromatogram

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® IF-3

250 x 4.6mm / 3µm

Mobile Phase Composition

ethanol / methanol / diethylamine = 70 / 30 / 0.1

Chromatographic Mode

Normal Phase

Flow rate (ml/min)

0.7

Injection amount (mg)

Temperature (°C)

25

Pressure (MPa)

Detection

UV 275 nm

Elution order

No.

Rt

K’

1

9.9

2

11.2

Alpha Value

Resolution

1 - 2

3.02

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