APPLICATION ID 1669

Bortezomib

COMPOUND IDENTIFICATION

Compound Name Bortezomib
Bortezomib

CHROMATOGRAM

Chromatogram

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® AD-3

250 x 4.6mm / 3µm

Mobile Phase Composition

n-heptane / ethanol / 2-propanol / formic acid = 90 / 5 / 5 / 0.1

Chromatographic Mode

Normal Phase

Flow rate (ml/min)

1.0

Injection amount (mg)

Temperature (°C)

25

Pressure (MPa)

Detection

UV 270 nm

Elution order

No.

Rt

K’

1

8.2

2

9.8

3

11.3

4

13.7

Alpha Value

Resolution

1 - 2

2.7

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