APPLICATION ID 1713

Ibrutinib

COMPOUND IDENTIFICATION

Compound Name Ibrutinib
Ibrutinib

CHROMATOGRAM

Chromatogram

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK ® IG

250 x 4.6mm / 5µm

Mobile Phase Composition

methanol / acetonitrile / ethylenediamine = 50 / 50 / 0.3

Chromatographic Mode

Normal Phase

Flow rate (ml/min)

1.0

Injection amount (mg)

Temperature (°C)

40

Pressure (MPa)

Detection

UV 258 nm

Elution order

No.

Rt

K’

1

6.2

2

10.4

Alpha Value

Resolution

1 - 2

10.4

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