APPLICATION ID 1747

Saxagliptin

COMPOUND IDENTIFICATION

Compound Name Saxagliptin
Saxagliptin

CHROMATOGRAM

Chromatogram

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® IG-3

250 x 4.6mm / 3µm

Mobile Phase Composition

ethanol / acetonitrile / isopropylamine = 20 / 80 / 0.1

Chromatographic Mode

Polar Phase

Flow rate (ml/min)

1.0

Injection amount (mg)

Temperature (°C)

25

Pressure (MPa)

Detection

UV 220 nm

Elution order

No.

Rt

K’

1

6.2

2

11.8

3

13.1

4

15.1

Alpha Value

Resolution

1 - 2

14.1

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