APPLICATION ID 226

N-CBZ-DL-Phenylalanine

COMPOUND IDENTIFICATION

Compound Name N-CBZ-DL-Phenylalanine
N-CBZ-DL-Phenylalanine

CHROMATOGRAM

Chromatogram

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® IB-3

150 x 4.6mm / 3µm

Mobile Phase Composition

n-hexane / chloroform / ethanol / trifluoroacetic acid = 68 / 30 / 2 / 0.1

Chromatographic Mode

Normal Phase
Secondary screening solvent (Immobilised CSP)

Flow rate (ml/min)

1

Injection amount (mg)

0.005

Temperature (°C)

25

Pressure (MPa)

Detection

UV 254 nm

Elution order

No.

Rt

K’

1

4.28

1.36

2

4.82

1.65

Alpha Value

Resolution

1 - 2

1.22

3.27

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