APPLICATION ID 432

Rosuvastatin (racemic)

COMPOUND IDENTIFICATION

Compound Name Rosuvastatin (racemic)
Rosuvastatin (racemic)

CHROMATOGRAM

Chromatogram

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® IB

250 x 4.6mm / 5µm

Mobile Phase Composition

n-hexane / ethanol / 2-propanol / trifluoroacetic acid = 90 / 5 / 5 / 0.3

Chromatographic Mode

Normal Phase
Primary screening solvent (Immobilised CSP)

Flow rate (ml/min)

1

Injection amount (mg)

Temperature (°C)

25

Pressure (MPa)

Detection

UV 250 nm

Elution order

No.

Rt

K’

1

17.72

4.91

2

20.44

5.81

Alpha Value

Resolution

1 - 2

1.18

2.3

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