APPLICATION ID 460

Valsartan (racemic)

COMPOUND IDENTIFICATION

Compound Name Valsartan (racemic)
Valsartan (racemic)

CHROMATOGRAM

Chromatogram

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® IC

250 x 4.6mm / 5µm

Mobile Phase Composition

n-hexane / ethanol / trifluoroacetic acid = 85 / 15 / 0.1

Chromatographic Mode

Normal Phase
Primary screening solvent (Immobilised CSP)

Flow rate (ml/min)

1

Injection amount (mg)

Temperature (°C)

25

Pressure (MPa)

Detection

UV 230 nm

Elution order

No.

Rt

K’

1

8.82

1.94

2

10.43

2.48

Alpha Value

Resolution

1 - 2

1.28

3.61

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