APPLICATION ID 987

Vildagliptin (racemic)

COMPOUND IDENTIFICATION

Compound Name Vildagliptin (racemic)
Vildagliptin (racemic)

CHROMATOGRAM

Chromatogram

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® IC

250 x 4.6mm / 5µm

Mobile Phase Composition

ethanol / diethylamine = 100 / 0.1

Chromatographic Mode

Polar Phase

Flow rate (ml/min)

0.5

Injection amount (mg)

Temperature (°C)

25

Pressure (MPa)

Detection

UV 210 nm

Elution order

No.

Rt

K’

1

11.32

0.89

2

14.34

1.39

Alpha Value

Resolution

1 - 2

1.57

4.02

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