化合物情報
クロマトグラム
分析レポート
|
カラム名 (カラムサイズ / 粒子径) |
CROWNPAK® CR-I(+) (3 x 150 mm 5 µm) |
|---|---|
| 移動相モード | HILIC |
| 移動相 | acetonitrile / ethanol / water / trifluoroacetic acid = 80 / 15 / 5 / 0.5 |
| 流速 (mL/min) | 0.4 | 温度 (℃) | 30 |
|---|---|---|---|
| 注入量 (µL) | サンプル濃度 | ||
| 検出器 | LC-MS | ||
| 溶出順序 | |||
| No. | Rt | K' |
|---|---|---|
| 1 | 1.6 | - |
| 2 | 3.0 |
| Alpha Value | Resolution | |
|---|---|---|
| 1 - 2 | - | 11.39 |
References；
Novel high-throughput and widely-targeted liquid chromatography–time of flight mass spectrometry method for d-amino acids in foods
Yutaka Konya, Moyu Taniguchi, Eiichiro Fukusaki
Volume 123, Issue 1, January 2017, Pages 126-133